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Effects of Different Extraction Methods on Vanilla Aroma.
Molecules. 2022 Jul 19; 27(14)M

Abstract

To establish the analytic conditions for examining the aroma quality of vanilla pods, we compared different extraction methods and identified a suitable option. We utilized headspace solid-phase microextraction (HS-SPME), steam distillation (SD), simultaneous steam distillation (SDE) and alcoholic extraction combined with gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) to identify volatile components of vanilla pods. A total of 84 volatile compounds were identified in this experiment, of which SDE could identify the most volatile compounds, with a total of 51 species, followed by HS-SPME, with a total of 28 species. Ten volatile compounds were identified by extraction with a minimum of 35% alcohol. HS-SPME extraction provided the highest total aroma peak areas, and the peak areas of aldehydes, furans, alcohols, monoterpenes and phenols compounds were several times higher than those of the other extraction methods. The results showed that the two technologies, SDE and HS-SPME, could be used together to facilitate analysis of vanilla pod aroma.

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Authors+Show Affiliations

Yeh CH
Taoyuan District Agricultural Research and Extension Station, Council of Agriculture, Executive Yuan, Taoyuan 327, Taiwan.
Chou CY
Taoyuan District Agricultural Research and Extension Station, Council of Agriculture, Executive Yuan, Taoyuan 327, Taiwan.
Wu CS
Department of Pharmacy, China Medical University Hospital, Taichung 404, Taiwan.
Chu LP
Department of Orthopedics, China Medical University Hospital, Taichung 404, Taiwan.
Huang WJ
Department of Cosmeceutics, China Medical University, Taichung 406, Taiwan.
Chen HC
Department of Cosmeceutics, China Medical University, Taichung 406, Taiwan.

MeSH

Gas Chromatography-Mass SpectrometryOdorantsSolid Phase MicroextractionSteamVanillaVolatile Organic Compounds

Pub Type(s)

Journal Article

Language

eng

PubMed ID

35889468

Citation

Yeh, Chih-Hsin, et al. "Effects of Different Extraction Methods On Vanilla Aroma." Molecules (Basel, Switzerland), vol. 27, no. 14, 2022.
Yeh CH, Chou CY, Wu CS, et al. Effects of Different Extraction Methods on Vanilla Aroma. Molecules. 2022;27(14).
Yeh, C. H., Chou, C. Y., Wu, C. S., Chu, L. P., Huang, W. J., & Chen, H. C. (2022). Effects of Different Extraction Methods on Vanilla Aroma. Molecules (Basel, Switzerland), 27(14). https://doi.org/10.3390/molecules27144593
Yeh CH, et al. Effects of Different Extraction Methods On Vanilla Aroma. Molecules. 2022 Jul 19;27(14) PubMed PMID: 35889468.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Effects of Different Extraction Methods on Vanilla Aroma. AU - Yeh,Chih-Hsin, AU - Chou,Chia-Yi, AU - Wu,Chin-Sheng, AU - Chu,Lee-Ping, AU - Huang,Wei-Juan, AU - Chen,Hsin-Chun, Y1 - 2022/07/19/ PY - 2022/06/24/received PY - 2022/07/12/revised PY - 2022/07/17/accepted PY - 2022/7/27/entrez PY - 2022/7/28/pubmed PY - 2022/7/29/medline KW - GC-MS KW - HS-SPME KW - SDE KW - vanilla KW - volatile components JF - Molecules (Basel, Switzerland) JO - Molecules VL - 27 IS - 14 N2 - To establish the analytic conditions for examining the aroma quality of vanilla pods, we compared different extraction methods and identified a suitable option. We utilized headspace solid-phase microextraction (HS-SPME), steam distillation (SD), simultaneous steam distillation (SDE) and alcoholic extraction combined with gas chromatography (GC) and gas chromatography-mass spectrometry (GC-MS) to identify volatile components of vanilla pods. A total of 84 volatile compounds were identified in this experiment, of which SDE could identify the most volatile compounds, with a total of 51 species, followed by HS-SPME, with a total of 28 species. Ten volatile compounds were identified by extraction with a minimum of 35% alcohol. HS-SPME extraction provided the highest total aroma peak areas, and the peak areas of aldehydes, furans, alcohols, monoterpenes and phenols compounds were several times higher than those of the other extraction methods. The results showed that the two technologies, SDE and HS-SPME, could be used together to facilitate analysis of vanilla pod aroma. SN - 1420-3049 UR - https://www.unboundmedicine.com/medline/citation/35889468/Effects_of_Different_Extraction_Methods_on_Vanilla_Aroma_ DB - PRIME DP - Unbound Medicine ER -