Tags

Type your tag names separated by a space and hit enter

Multiresidue gas chromatographic method for determining organochlorine pesticides in poultry fat: collaborative study.
J Assoc Off Anal Chem. 1984 Mar-Apr; 67(2):284-9.JA

Abstract

A gas chromatographic electron capture detector method is described for the quantitative determination of organochlorine pesticide residues in poultry fat. The samples are rendered and cleaned up using automated gel permeation chromatography. The collaborative samples consisted of 10 fortified samples and one incurred residue sample, all in duplicate. Fortification levels ranged from 0.15 to 1.0 ppm for alpha-BHC, lindane, cis- and trans-chlordane, octachlor epoxide, o,p' and p,p'-DDT, p,p'-DDE, p,p'-TDE, hexachlorobenzene, heptachlor epoxide, dieldrin, endrin, methoxychlor, mirex, and toxaphene. The average recovery was 91.9% with a range of 81-102%. The ranges of coefficients of variation were: CVo = 3.39-14.79%; CVL = 0-16.6%; and CVx = 5.82-19.0%. The results indicate accuracy and precision comparable to other official methodology. The method has been adopted official first action.

Authors

No affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

6725198

Citation

Ault, J A., and T E. Spurgeon. "Multiresidue Gas Chromatographic Method for Determining Organochlorine Pesticides in Poultry Fat: Collaborative Study." Journal - Association of Official Analytical Chemists, vol. 67, no. 2, 1984, pp. 284-9.
Ault JA, Spurgeon TE. Multiresidue gas chromatographic method for determining organochlorine pesticides in poultry fat: collaborative study. J Assoc Off Anal Chem. 1984;67(2):284-9.
Ault, J. A., & Spurgeon, T. E. (1984). Multiresidue gas chromatographic method for determining organochlorine pesticides in poultry fat: collaborative study. Journal - Association of Official Analytical Chemists, 67(2), 284-9.
Ault JA, Spurgeon TE. Multiresidue Gas Chromatographic Method for Determining Organochlorine Pesticides in Poultry Fat: Collaborative Study. J Assoc Off Anal Chem. 1984 Mar-Apr;67(2):284-9. PubMed PMID: 6725198.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Multiresidue gas chromatographic method for determining organochlorine pesticides in poultry fat: collaborative study. AU - Ault,J A, AU - Spurgeon,T E, PY - 1984/3/1/pubmed PY - 1984/3/1/medline PY - 1984/3/1/entrez SP - 284 EP - 9 JF - Journal - Association of Official Analytical Chemists JO - J Assoc Off Anal Chem VL - 67 IS - 2 N2 - A gas chromatographic electron capture detector method is described for the quantitative determination of organochlorine pesticide residues in poultry fat. The samples are rendered and cleaned up using automated gel permeation chromatography. The collaborative samples consisted of 10 fortified samples and one incurred residue sample, all in duplicate. Fortification levels ranged from 0.15 to 1.0 ppm for alpha-BHC, lindane, cis- and trans-chlordane, octachlor epoxide, o,p' and p,p'-DDT, p,p'-DDE, p,p'-TDE, hexachlorobenzene, heptachlor epoxide, dieldrin, endrin, methoxychlor, mirex, and toxaphene. The average recovery was 91.9% with a range of 81-102%. The ranges of coefficients of variation were: CVo = 3.39-14.79%; CVL = 0-16.6%; and CVx = 5.82-19.0%. The results indicate accuracy and precision comparable to other official methodology. The method has been adopted official first action. SN - 0004-5756 UR - https://www.unboundmedicine.com/medline/citation/6725198/Multiresidue_gas_chromatographic_method_for_determining_organochlorine_pesticides_in_poultry_fat:_collaborative_study_ L2 - https://antibodies.cancer.gov/detail/CPTC-Ezrin-2 DB - PRIME DP - Unbound Medicine ER -