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Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry.
J Forensic Sci. 1984 Apr; 29(2):611-7.JF

Abstract

A detailed procedure of an extremely sensitive method for quantitation of methamphetamine and amphetamine in human hair by gas chromatography (GC)/chemical ionization (CI) mass spectrometry (MS) is presented. N-methylbenzylamine was used as an internal standard. The samples, after extraction with an organic solvent, were derivatized with trifluoroacetic anhydride before the GC/MS analysis. Quantitation was made with quasi-molecular ions of the derivatives by selected ion monitoring in the CI mode. The detection limit was about 10 pg in an injected volume. The high sensitivity enabled us to measure both stimulants in a single human hair in actual cases.

Authors

No affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

6726166

Citation

Suzuki, O, et al. "Detection of Methamphetamine and Amphetamine in a Single Human Hair By Gas Chromatography/chemical Ionization Mass Spectrometry." Journal of Forensic Sciences, vol. 29, no. 2, 1984, pp. 611-7.
Suzuki O, Hattori H, Asano M. Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry. J Forensic Sci. 1984;29(2):611-7.
Suzuki, O., Hattori, H., & Asano, M. (1984). Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry. Journal of Forensic Sciences, 29(2), 611-7.
Suzuki O, Hattori H, Asano M. Detection of Methamphetamine and Amphetamine in a Single Human Hair By Gas Chromatography/chemical Ionization Mass Spectrometry. J Forensic Sci. 1984;29(2):611-7. PubMed PMID: 6726166.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Detection of methamphetamine and amphetamine in a single human hair by gas chromatography/chemical ionization mass spectrometry. AU - Suzuki,O, AU - Hattori,H, AU - Asano,M, PY - 1984/4/1/pubmed PY - 1984/4/1/medline PY - 1984/4/1/entrez SP - 611 EP - 7 JF - Journal of forensic sciences JO - J Forensic Sci VL - 29 IS - 2 N2 - A detailed procedure of an extremely sensitive method for quantitation of methamphetamine and amphetamine in human hair by gas chromatography (GC)/chemical ionization (CI) mass spectrometry (MS) is presented. N-methylbenzylamine was used as an internal standard. The samples, after extraction with an organic solvent, were derivatized with trifluoroacetic anhydride before the GC/MS analysis. Quantitation was made with quasi-molecular ions of the derivatives by selected ion monitoring in the CI mode. The detection limit was about 10 pg in an injected volume. The high sensitivity enabled us to measure both stimulants in a single human hair in actual cases. SN - 0022-1198 UR - https://www.unboundmedicine.com/medline/citation/6726166/Detection_of_methamphetamine_and_amphetamine_in_a_single_human_hair_by_gas_chromatography/chemical_ionization_mass_spectrometry_ L2 - https://medlineplus.gov/methamphetamine.html DB - PRIME DP - Unbound Medicine ER -