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High performance liquid chromatography of furfural and hydroxymethylfurfural in spirits and honey.
J Assoc Off Anal Chem. 1980 Nov; 63(6):1215-8.JA

Abstract

Furfural (2-furaldehyde) and hydroxymethylfurfural (5-hydroxy-2-furaldehyde, HMF) are determined in brandy and honey by reverse phase high performance liquid chromatography. Brandies and other spirits are injected without sample preparation; honey is diluted with water and the solution is filtered before injection onto a reverse phase column with detection at 285 nm. The mobile phase is methanol--water (10 + 90) and the effluent flow rate is maintained at 1.0 mL/min. External standardization is used for quantitative determination. Recoveries from cognac and honey spiked at different levels ranged from 95 to 99% (furfural) and 95 to 100% (HMF). The furfural content of the brandies was also determined by the existing colorimetric method of the Bureau National Interprofessionel du Cognac. The HMF content of the honey was correlated to the results of the classic method of Winkler.

Authors

No affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

7451383

Citation

Jeuring, H J., and F J. Kuppers. "High Performance Liquid Chromatography of Furfural and Hydroxymethylfurfural in Spirits and Honey." Journal - Association of Official Analytical Chemists, vol. 63, no. 6, 1980, pp. 1215-8.
Jeuring HJ, Kuppers FJ. High performance liquid chromatography of furfural and hydroxymethylfurfural in spirits and honey. J Assoc Off Anal Chem. 1980;63(6):1215-8.
Jeuring, H. J., & Kuppers, F. J. (1980). High performance liquid chromatography of furfural and hydroxymethylfurfural in spirits and honey. Journal - Association of Official Analytical Chemists, 63(6), 1215-8.
Jeuring HJ, Kuppers FJ. High Performance Liquid Chromatography of Furfural and Hydroxymethylfurfural in Spirits and Honey. J Assoc Off Anal Chem. 1980;63(6):1215-8. PubMed PMID: 7451383.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - High performance liquid chromatography of furfural and hydroxymethylfurfural in spirits and honey. AU - Jeuring,H J, AU - Kuppers,F J, PY - 1980/11/1/pubmed PY - 1980/11/1/medline PY - 1980/11/1/entrez SP - 1215 EP - 8 JF - Journal - Association of Official Analytical Chemists JO - J Assoc Off Anal Chem VL - 63 IS - 6 N2 - Furfural (2-furaldehyde) and hydroxymethylfurfural (5-hydroxy-2-furaldehyde, HMF) are determined in brandy and honey by reverse phase high performance liquid chromatography. Brandies and other spirits are injected without sample preparation; honey is diluted with water and the solution is filtered before injection onto a reverse phase column with detection at 285 nm. The mobile phase is methanol--water (10 + 90) and the effluent flow rate is maintained at 1.0 mL/min. External standardization is used for quantitative determination. Recoveries from cognac and honey spiked at different levels ranged from 95 to 99% (furfural) and 95 to 100% (HMF). The furfural content of the brandies was also determined by the existing colorimetric method of the Bureau National Interprofessionel du Cognac. The HMF content of the honey was correlated to the results of the classic method of Winkler. SN - 0004-5756 UR - https://www.unboundmedicine.com/medline/citation/7451383/High_performance_liquid_chromatography_of_furfural_and_hydroxymethylfurfural_in_spirits_and_honey_ L2 - https://www.lens.org/lens/search/patent/list?q=citation_id:7451383 DB - PRIME DP - Unbound Medicine ER -