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Capillary electrophoretic separation of TNT and its transformation products.
J Capillary Electrophor. 1996 Jul-Aug; 3(4):209-13.JC

Abstract

2,4,6-Trinitrotoluene (TNT), 2-aminodinitrotoluene (2ADNT), 4-aminodinitrotoluene (4ADNT), and diamino-6-nitrotoluene (DA6NT) in a variety of matrices (including chemical, microbial, and plant extract) were successfully separated and quantified using micellar electrokinetic capillary electrophoresis (MEKC). The method used a buffer solution of 20 mM in borax, 50 mM in sodium dodecyl sulfate (SDS), and of pH 8.5. Voltage applied across the capillary was 20 kV and temperature was maintained at 25 degrees C. Compounds eluted within approximately 6-11 min and were identified by both their migration times and spectra.

Authors+Show Affiliations

Pucik L
SECOR Geochemistry, Sacramento, CA 95815-4404, USA.
Hughes J
No affiliation info available

MeSH

Aniline CompoundsAutomationElectrophoresis, CapillaryIndicators and ReagentsMicellesPlant ExtractsReproducibility of ResultsSensitivity and SpecificityToluidinesTrinitrotoluene

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

9384739

Citation

Pucik, L, and J Hughes. "Capillary Electrophoretic Separation of TNT and Its Transformation Products." Journal of Capillary Electrophoresis, vol. 3, no. 4, 1996, pp. 209-13.
Pucik L, Hughes J. Capillary electrophoretic separation of TNT and its transformation products. J Capillary Electrophor. 1996;3(4):209-13.
Pucik, L., & Hughes, J. (1996). Capillary electrophoretic separation of TNT and its transformation products. Journal of Capillary Electrophoresis, 3(4), 209-13.
Pucik L, Hughes J. Capillary Electrophoretic Separation of TNT and Its Transformation Products. J Capillary Electrophor. 1996 Jul-Aug;3(4):209-13. PubMed PMID: 9384739.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Capillary electrophoretic separation of TNT and its transformation products. AU - Pucik,L, AU - Hughes,J, PY - 1996/7/1/pubmed PY - 1997/12/31/medline PY - 1996/7/1/entrez SP - 209 EP - 13 JF - Journal of capillary electrophoresis JO - J Capillary Electrophor VL - 3 IS - 4 N2 - 2,4,6-Trinitrotoluene (TNT), 2-aminodinitrotoluene (2ADNT), 4-aminodinitrotoluene (4ADNT), and diamino-6-nitrotoluene (DA6NT) in a variety of matrices (including chemical, microbial, and plant extract) were successfully separated and quantified using micellar electrokinetic capillary electrophoresis (MEKC). The method used a buffer solution of 20 mM in borax, 50 mM in sodium dodecyl sulfate (SDS), and of pH 8.5. Voltage applied across the capillary was 20 kV and temperature was maintained at 25 degrees C. Compounds eluted within approximately 6-11 min and were identified by both their migration times and spectra. SN - 1079-5383 UR - https://www.unboundmedicine.com/medline/citation/9384739/Capillary_electrophoretic_separation_of_TNT_and_its_transformation_products_ DB - PRIME DP - Unbound Medicine ER -